On-line titration using colorimetric end point detection

Optics: measuring and testing – For light transmission or absorption – Of fluent material

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Details

356246, 356338, 250576, G01N 2100, G01N 110

Patent

active

051810824

ABSTRACT:
Radiant energy is transmitted to a probe element including an interior conical reflecting surface and a fluid sample chamber. Portions of the light which have been transmitted, partially attenuated, or scattered by a fluid sample in the sample chamber are directed by at least a portion of the interior conical reflecting surface to means for collecting the transmitted, partially attenuated, or scattered light. A stilling valve incorporated into the probe element enables elimination of entrained gas bubbles from the chamber. A specific application of the probe is disclosed in which a titration analyzer is combined with electro-optic signal conversion and processing circuits and a probe according to the invention to provide titration colorimetric endpoint determination in measuring the free fatty acid content of a fluid such as a edible oil or fat.

REFERENCES:
patent: 3734621 (1973-05-01), Moody et al.
patent: 3746452 (1973-07-01), Teboul et al.
patent: 4807630 (1989-02-01), Malinouskas
patent: 4843247 (1989-06-01), Yamazoe et al.
patent: 5007740 (1991-04-01), Jeannotte et al.
"FFA Determination Using an On-Line Titrator and a Colorimetric Sensor", by C. Cheney et al., paper presented at Sensors Epox West, May 1989.
"Construction and Performance of a Fluorimetric Acid-Base Titrator with a Blue LED as a Light Source", O. S. Wolbeis et al.; Analyst, Nov. 1986, pp. 1331-1334.

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