Obtaining caprolactam from epsilon-aminocaproic acid

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D20108

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active

045991995

ABSTRACT:
Caprolactam is obtained by treating .epsilon.-aminocaproic acid with steam at elevated temperatures in the presence of a catalyst by a process in whcih .epsilon.-aminocaproic acid is introduced into a fluidized alumina bed and treated in the presence of steam at from 290.degree. to 400.degree. C.

REFERENCES:
patent: 2956051 (1960-10-01), Duxbury et al.
patent: 3658810 (1972-04-01), Tanaka et al.
patent: 3988319 (1976-10-01), Mares
patent: 4360461 (1982-11-01), Fuchs et al.
Tetrahedron Letters vol. 21, pp. 2443-2446.

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