Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...
Patent
1985-02-15
1985-11-12
Raymond, Richard L.
Organic compounds -- part of the class 532-570 series
Organic compounds
Heterocyclic carbon compounds containing a hetero ring...
C07F 965
Patent
active
045529680
ABSTRACT:
A process for preparing N-phosphonomethylglycine which comprises:
(1) reacting a primary amine with formaldehyde to produce N,N',N"-tris-substituted-hexahydro-s-triazine;
(2) reacting the triazine with an haloacetyl halide, preferably chloroacetyl chloride, to form the N-(substituted)-N-halomethyl acetamide of the haloacetyl halide;
(3) reacting the amide with O,O-di-(substituted)-aminomethylphosphonate to form O,O-di-(substituted)-1-phosphonomethyl-3-(substituted)-1,3-imidazol-4-one; and
(4) hydrolyzing the 1,3-imadazol-4-one to yield N-phosphonomethylglycine.
REFERENCES:
patent: 3925406 (1975-12-01), Porret et al.
Baker Edwin H.
Raymond Richard L.
Stauffer Chemical Company
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