Novel process for synthesis of a liquid irritant, 1-methoxycyclo

Details Novel process for synthesis of a liquid irritant, 1-methoxycyclo Novel process for synthesis of a liquid irritant, 1-methoxycyclo

1978-04-28

1981-02-03

Sebastian, Leland A.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

424339, C07C 4106

Patent

active

042490251

ABSTRACT:
An improved multi-step process for synthesizing the liquid irritant 1-metycycloheptatriene from tropylium tetrafluoborate the improvement comprising the step of using a polymerization/condensation inhibitor or retarder to minimize impurities and increase yield of the irritant product. Phenothiazine is the preferred polymerization inhibitor.

REFERENCES:
patent: 3084194 (1963-03-01), ter Borg et al.

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