Electricity: measuring and testing – Particle precession resonance – Spectrometer components
Patent
1995-10-17
1996-09-03
Arana, Louis M.
Electricity: measuring and testing
Particle precession resonance
Spectrometer components
324318, G01V 300
Patent
active
055527094
ABSTRACT:
The present invention relates to improving the sensitivity of an NMR system for electrically conductive (polar) NMR samples. Many NMR samples use water or a salt solution of water or other electrically conductive liquid as a solvent for biologically active materials. When such a sample is placed in the probe coil of an NMR spectrometer, electrical losses in the conductive material lowers the Q of the receiving circuit and thereby reduces the sensitivity of the spectrometer. These electrical losses can be greatly reduced by breaking up the current paths within the sample. This can be achieved by a special sample cell that compartmentalizes the sample with electrical insulating material reducing the electrical current paths.
REFERENCES:
patent: 4551678 (1985-11-01), Morgan et al.
patent: 5469061 (1995-11-01), Linehan et al.
"Multi-Cloistered" NMR Cells by E. M. Banas, Applied Spectroscopy, vol. 23 No. 1 1969 pp. 281-282.
Arana Louis M.
Berkowitz Edward
Fisher Gerald M.
Varian Associates Inc.
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