NMR CryoMAS probe for high-field wide-bore magnets

Details NMR CryoMAS probe for high-field wide-bore magnets NMR CryoMAS probe for high-field wide-bore magnets

2011-03-29

2011-03-29

Shrivastav, Brij B (Department: 2858)

Electricity: measuring and testing

Particle precession resonance

Spectrometer components

C324S321000

Reexamination Certificate

active

07915893

ABSTRACT:
All critical circuit components, including the sample coils, are located along with the spinner assembly in a region that may be evacuated to high vacuum for thermal insulation and high-voltage operation. A hermetically sealed spinner assembly simultaneously satisfies the requirements of hermeticity, low total emissivity, rf compatibility, spinning performance, magnetic compatibility, and high filling factor by utilizing metal construction except for the central region near the rf sample coils. Hence, it is possible to maintain high vacuum in the region external to the MAS spinner assembly even over a broad range of bearing and drive gas temperatures. A bundle of optical fibers is provided for tachometry for spin rates up to 60 kHz. The use of alumina disc capacitors allows the noise contributions from the most critical capacitors to be reduced to a minor fraction of the total and simplifies high voltage operation.

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