Nitrogen rejection method and apparatus

Refrigeration – Cryogenic treatment of gas or gas mixture – Separation of gas mixture

Reexamination Certificate

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C062S927000

Reexamination Certificate

active

07059152

ABSTRACT:
Nitrogen is rejected from a feed natural gas stream comprising methane and nitrogen so as to form a primary methane product. The mole fraction of nitrogen in the feed natural gas increases over a period of time. The feed natural gas stream is cooled in a main heat exchanger and is rectified in a double rectification column. A primary product methane stream and a secondary nitrogen-enriched product stream are withdrawn from the rectification column. The secondary nitrogen-enriched product stream has a mole fraction of methane at or above a chosen minimum value when the said mole fraction of nitrogen is at a minimum. When the said mole fraction of nitrogen rises to a value at which the mole fraction of methane in the secondary nitrogen-enriched product stream falls below the chosen minimum, a part of the feed gas is introduced through conduit into the secondary nitrogen-enriched product stream so as to restore its mole fraction of methane to the chosen minimum value or a value thereabove.

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Craig A. Pruitt, J. V. O'Brien; “Wyoming's Shute Creek Plant Uses NRU Unit,” Oil & Gas Journal, Oct. 9, 1989, pp. 78-82.

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