Nitration of alkanols

Details Nitration of alkanols Nitration of alkanols

1988-04-06

1992-11-10

Kyle, Deborah L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrate esters or chalcogen analogues thereof

C07C20304

Patent

active

051625687

ABSTRACT:
A process for nitrating alkanols containing 5-13 carbon atoms is disclosed. The nitation takes place at 15.degree.-45.degree. C. using a mixed acid containing 20-30% nitric acid, 55-60% sulfuric acid and 15-20% water, and 2-5%, based on mixed acid, of a stabilizer selected from the class consisting of urea, sulfamic acid and hydrazine.

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patent: 4420311 (1983-12-01), Thomas
N. N. Lebedev, Chemistry and Technology of Basic Organic and Petrochemical Synthesis, 1981, (English Translation, 1984), pp. 369-371.

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