Nickel-iron (80:20) alloy thin film electroplating method and el

Chemistry: electrical and wave energy – Processes and products

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204123, 204239, 204273, 204274, C25D 356, C25C 124, C25D 2114

Patent

active

041027566

ABSTRACT:
A thin film of low magnetostriction Permalloy 80% nickel - 20% iron .+-. 1% is electroplated in a bath having a ratio of about 1.8:1 to 24:1 g/liter ratio of Ni to Fe ions with a plating current density from 10 ma/cm.sup.2 - 200 ma/cm.sup.2 when plating in sheet form or an Ni/Fe ratio of 25:1 to 85:1 with a current density of 2 ma/cm.sup.2 - 110 ma/cm.sup.2 when plating through a mask. The fluid in the system is constantly mixed, replenished with fresh iron, acid, and other reagents, is adjusted in temperature and subjected to a continuous laminar regime of mixing. Fresh solution is added to the bath from a reservoir where the above adjustments are made. The inlet for the fresh solution is at the lower end of the plating chamber and directed at a bath mixer which includes a slot through which the fresh solution is directed to optimize mixing in the plating chamber. Complexing agents are avoided. High speed plating is obtained with about 24.4 g/l of Ni.sup.++, 1.05 g/l of Fe.sup.++, 25 g/l of H.sub.3 BO.sub.3, 0.2 g/l of Na saccharin and a pH of 1.5 to 3.6.

REFERENCES:
patent: 3317410 (1967-05-01), Croll et al.
patent: 3434956 (1969-03-01), Glenn
patent: 3442774 (1969-05-01), Mehaute et al.
patent: 3649509 (1972-03-01), Morawetz et al.

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