Ni and Ni/NiO core-shell nanoparticles

Specialized metallurgical processes – compositions for use therei – Processes – Producing or purifying free metal powder or producing or...

Reexamination Certificate

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C075S374000, C423S594190

Reexamination Certificate

active

07601199

ABSTRACT:
Glycerol is used as a solvent medium for the precipitation of a complex of nickel and glycerol material. The precipitate is separated from the liquid solvent and dried and calcined in air to produce small (nanometer size) particles characterized by a nickel core encased in a nickel oxide shell. The proportions of nickel core and nickel oxide shell can be controlled by management of the time and temperature of heating in air. Prolonged heating in air can produce nickel oxide particles, or calcining of the precipitate in nitrogen produces nickel particles.

REFERENCES:
patent: 4539041 (1985-09-01), Figlarz et al.
patent: 5512094 (1996-04-01), Linton
patent: 1381328 (2002-11-01), None
patent: 1415621 (2003-05-01), None
patent: 1631589 (2005-06-01), None
Korean Office Action; translation and original document.

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