Nano-crystal austenitic steel bulk material having...

Specialized metallurgical processes – compositions for use therei – Compositions – Consolidated metal powder compositions

Reexamination Certificate

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C075S232000, C075S244000

Reexamination Certificate

active

07662207

ABSTRACT:
The invention provides a super hard and tough, nano-crystal austenite steel bulk material having an improved corrosion resistance, and its preparation process.The austenite steel bulk material comprises an aggregate of austenite nano-crystal grains containing 0.1 to 2.0% (by mass) of a solid solution type nitrogen, wherein an oxide, nitride, carbide or the like of a metal or semimetal exists as a crystal grain growth inhibitor between and/or in said nano-crystal grains.For preparation, fine powders of austenite steel-forming components, i.e., iron and chromium, nickel, manganese, carbon or the like are mixed with a substance that becomes a nitrogen source. Mechanical alloying (MA) is applied to the mixture, thereby preparing nano-crystal austenite steel powders having a high nitrogen concentration. Finally, the austenite steel powders are consolidated by sintering by means of spark plasma sintering, rolling or the like.

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Current Advances in Materials and Processes, vol. 15, No. 3, (2002), pp. 454 to 457.
Current Advances in Materials and Processes, vol. 13, No. 3, (2002), pp. 362 to 363.
Harumatsu Miura, “Mechanical Alloying ni yori Sakusei shita Kochiso Nano Kessho Austentite Stainless-ko Funmatsu no Neddan Koka Seikei Katei deno Chisso no Kyodo”, Current Advances in Materials and Processes, vol. 15, No. 3, (2002), pp. 454 to 457.
Harumatsu Miura, “Mechanical Alloying ni yotte Sakusei shita Kochiso Stainless-ko Funmatsu no Austentite-ka to Koka Seikei”, Current Advances in Materials and Processes, vol. 13, No. 3, (2000), pp. 362 to 363.
Harumatsu Miura,, Preparation of Nanocrystalline High-Nitrogen Stainless Steel Powders by Mechanical Alloying and Their HotCompaction, Materials Transactions, vol. 42, No. 11, (2001), pp. 2368 to 2373.
Miura H et al, “Composition Dependence of Microstructure of Mechanically Alloyed Powders and Their Compacts of High Nitrogen CR-MN Steels”, Materials Transactions, Jim, Sendai, JP, vol. 40, No. 9, Sep. 1999, pp. 907-910.

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