Multistage countercurrent recrystallization process and apparatu

Chemistry: physical processes – Physical processes – Crystallization

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Details

23295R, 23302R, 23302T, 422254, 4234991, B91D 900, C01D 316

Patent

active

052404676

ABSTRACT:
A multistage process for the separation and purification of a desired crystalline material by repeated dissolution and recrystallization, wherein crystals and solvent move countercurrent to one another through the stages. A fluid temperature gradient is maintained within each recrystallization unit to make use of convection to facilitate or accelerate concurrent dissolution and recrystallization within a single vessel. Solid recrystallized material is moved from one unit to the next unit. An automated apparatus and a manually operated apparatus for carrying out the process are also described.

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