Compositions: ceramic – Ceramic compositions – Refractory
Patent
1988-10-25
1990-10-02
Dixon, Jr., William R.
Compositions: ceramic
Ceramic compositions
Refractory
501 5, 501127, 423328, C04B 3500
Patent
active
049607383
ABSTRACT:
A mullite-alumina composite sintered body composed of from 75 wt % to 85 wt % Al.sub.2 O.sub.3 balance SiO.sub.2, consisting of two crystalline phases, mullite and .alpha.-phase alumina, and being free from glass phase, wherein both of the average diameters of mullite grains and .alpha.-phase alumina grains are not more than 1.0 .mu.m, the content of grains having the longitudinal-length of not less than 2.5 .mu.m is 1% or less in the observation of a cross section of said sintered body, and the porosity of said sintered body is 1% or less.
The sintered body of the present invention is produced by a process comprising the steps of preparing a starting powdery material composed of from 75 wt % to 85 wt % Al.sub.2 O.sub.3 balance SiO.sub.2 and containing amorphous phase from 65 wt % to 90 wt %, wherein each particle of said starting powdery material contains both Al.sub.2 O.sub.3 and SiO.sub.2, and sintering said starting powdery material at a temperature in the range from 1500.degree. C. to 1650.degree. C.
The sintered body of the present invention has a high bending strength exceeding 500 MPa at room temperature.
REFERENCES:
patent: 3857923 (1974-12-01), Gardner et al.
patent: 4272500 (1981-06-01), Eggerding et al.
patent: 4418024 (1983-11-01), Prochzka et al.
patent: 4418025 (1983-11-01), Prochazka et al.
patent: 4640904 (1987-02-01), Hillig et al.
patent: 4774068 (1988-09-01), Hiraiwa et al.
Gani et al. "Glass Formation & Phase Transformations in Plasma Prepared Al.sub.2 O.sub.3 --SiO.sub.2 Powders" Journal of Natl. Sci. vol. 12 pp. 999-1009 (1977).
Kanzaki et al, "Dependency of Mechanical Property of Sintered Mullite on Chemical; Compositions", Yogyo-Kyokai-shi, vol. 93, No. 7, pp. 407-408 (1985).
Somiya, "Mullite", Uchida Rokakuho, pp. 51-61 (1985).
Ismail et al, "Microstructure and Mechanical Properties of Mullite Prepared by the Sol-Gel Method", J. Am. Ceram. Soc., vol. 70, No. 1, C-7-C-9 (1987).
Gardner et al, U.S. Pat. No. 3,857,923, "Mullite Package for Integrated Circuit Devices", Dec. 31, 1974.
Gani et al "Glass Formation and Phase Transformations in Plasma Prepared Al.sub.2 O.sub.3 --SiO.sub.2 Powders", Journal of Materials Science, vol. 12, pp. 999-1009 (1977).
Debely et al, "Preparation and Sintering Behavior of Fine-Grained Al.sub.2 O.sub.3 --SiO.sub.2 Composite", J. Am. Ceram. Soc., vol. 68, No. 3, C-76-C-78, (1985).
Okada et al, "Formation Reaction of Mullite from SiO.sub.2 --Al.sub.2 O.sub.3 Xerogels", Journal of Materials Science Letters, vol. 5, pp. 13-15-1318 (1986).
Cameron, "Composition and Cell Dimensions of Mullite", Ceramic Bulletin, vol. 56, No. 11, pp. 1003-1011 (1977).
Hori Saburo
Kurita Ryuichi
Dixon Jr. William R.
Gallo Chris
Kureha Chemical Industry Co. Ltd.
LandOfFree
Mullite-alumina composite sintered body and process for producin does not yet have a rating. At this time, there are no reviews or comments for this patent.
If you have personal experience with Mullite-alumina composite sintered body and process for producin, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Mullite-alumina composite sintered body and process for producin will most certainly appreciate the feedback.
Profile ID: LFUS-PAI-O-292409