Powder metallurgy processes – Powder metallurgy processes with heating or sintering – Metal and nonmetal in final product
Reexamination Certificate
2006-09-19
2006-09-19
Langel, Wayne A. (Department: 1754)
Powder metallurgy processes
Powder metallurgy processes with heating or sintering
Metal and nonmetal in final product
C423S440000
Reexamination Certificate
active
07108831
ABSTRACT:
The present invention relates to a method of producing tungsten carbide by gas phase direct carburization of a tungsten-oxide containing starting material, wherein the starting material is reacted with a reaction gas at an increased temperature. The starting material is first heated to a first temperature greater than or equal to 600° C., before reacting with a reaction gas while increasing the temperature to a second temperature that does not exceed 850° C., wherein the reaction gas is selected from the group consisting of CO and a COH2gas mixture comprising up to 20% by volume H2.
REFERENCES:
patent: 4049380 (1977-09-01), Yih et al.
patent: 5372797 (1994-12-01), Dunmead
patent: 5380688 (1995-01-01), Dunmead et al.
patent: 5885372 (1999-03-01), Seegopaul
patent: 6030912 (2000-02-01), Yamamoto et al.
patent: 2350576 (2000-05-01), None
patent: 0 834 589 (1998-04-01), None
patent: A 1 016 624 (2000-07-01), None
patent: 3252306 (1991-11-01), None
patent: WO A 93/10042 (1993-05-01), None
patent: 0029325 (2000-05-01), None
F. H. Ribeiro, R. A. Dalla Betta, G. J. Guskey, M. Boudart Preparation and surface composition of tungsten carbide powders with high specific surface area Chem. Mater.; 1991; 3(5): 805-812.
Deutsch Chemische Gesellschaft: “Gmelins Handbuch der anorganischen Chemie, System-Nr 54: Wolfram, Hauptband, 8. Auflage” 1933, Verlag Chemie GMBH, Weinheim, Seite 190, Zeile 2-10.
Erik Lassner, Wolf-Dieter Schubert, Tungsten Properties, Chemistry, Technology of the Element, Alloys and Chemical Compounds, Kluwer Academic, Plenum Publishers, New York 1999, pp. 88 109 and 330-331.
Qian, Chongliang and Wu, Enxi, “Phase transition of W-Co oxide mixture during deirect reduction/carburization by H2/CH4”, Transactions of Nfsoc, vol. 5, No. 3, 1995, pp. 554-560.
Alonso et al., “Tungsten trioxide reduction-carburization with carbon monoxide-carbon dioxide mixtures: kinetics and thermodynamics”, Internal Journal of Mineral Processing, 20, 1987, pp. 137-151.
Davidson et al., “Initial Kinetics of tungsten carburization by methane”, Metallurgic Transactions B. vol. 9B, 1978, pp. 553-557.
A.K. Basu and F.R. Sale, “A morphological study of the carburization/reduction of tungsten oxides with carbon monoxide”, Metallurgic Transactions B. vol. 9B, 1978, pp. 603-613.
“Ullmann's Encyclopedia of Industrial Chemistry”, 5th Edition, vol. A5, VCH: 65-68.
Eckhart Jürgen
Leitner Jürgen
Rabitsch Kurt
Baker & Botts LLP
Langel Wayne A.
Raetzsch Alvin T
Treibacher Industrie AG
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