Monomer and diluent recovery

Distillation: processes – separatory – Plural distillations performed on same material – One a distillation under positive pressure or vacuum

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203 77, 203 78, 203 82, 203 87, 203DIG19, 203 99, 526348, 159DIG18, B01D 300

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active

045899576

ABSTRACT:
Improved process for the separation of a hydrocarbon-containing feedstream comprising monomer, comonomer and diluent into separate product streams which comprises subjecting the feedstream to two-stage distillation provided with a common accumulation zone wherein the condensate from the accumulation zone serves as the source of feed for the second distillation and reflux for the first distillation. In a specific embodiment, a feed comprising ethylene, 1-hexene, and isobutane is separated into separate streams of 1-hexene, ethylene and isobutane, and isobutane for recycle to polymerization.

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