Mono carbonylation of benzene diols

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acid esters

Reexamination Certificate

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Reexamination Certificate

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06933403

ABSTRACT:
A process for a mono carbonylation of a benzenediol of the formula (I) is characterized in that a benzene diol of the formula (II) is reacted with an acid anhydride or carbonyl halide of the formula (III) without any organic or inorganic bases for thereby producing a monocarbonylated benzenediol of the formula (I):wherein R is hydrogen, C1-C15alkyl group, cycle alkyl group, aryl group, alkoxy group, aryloxy group, dialkylamino group, alkylarylamino group or diarylamino group, and X is a general leaving group such as fluoride, chloride, bromide, iodide, acetoxy, etc.

REFERENCES:
patent: 178929 (1986-04-01), None
patent: 62-249945 (1987-10-01), None
patent: 5-140035 (1993-06-01), None
Xia et al., “Study on Synthesis of 1,4-Benzenediol Monoacetate”, Journal of China University of Mining & Technology 2001: 30(6), 11-12.
Tangestaninejad et al., “Rapid and Efficient Acetylation of Alcohols and Phenols with Acetic Anhydride Using Tin(IV) Porphyrin as Catalyst”, Synthetic Communications, 2002: 32(9), 1337-1343.

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