Microliter-sized ionization device and method

Electricity: measuring and testing – Using ionization effects – For analysis of gas – vapor – or particles of matter

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Details

324 711, 250324, 250423R, 31323171, 73 234, G01N 2762

Patent

active

059558865

ABSTRACT:
A microliter-sized metastable ionization device with a cavity, a sample gas inlet, a corona gas inlet and a gas outlet. A first electrode has a hollow and disposed in the cavity and is in fluid communication with the sample gas inlet. A second electrode is in fluid communication with the corona gas inlet and is disposed around the first electrode adjacent the hollow end thereof. A gap forming means forms a corona gap between the first and second electrodes. A first power supply is connected to the first electrode and the second power supply is connected to the second electrode for generating a corona discharge across the corona gap. A collector has a hollow end portion disposed in the cavity which is in fluid communications with the gas outlet for the outgassing and detection of ionized gases. The first electrode can be a tubular member aligned concentrically with a cylindrical second electrode. The gap forming means can be in annular disc projecting radially inwardly from the cylindrical second electrode. The collector can have a tubular opening aligned coaxially with the first electrode and has an end face spaced a short distance from an end face of the first electrode forming a small active volume therebetween for the generation and detection of small quantities of trace analytes.

REFERENCES:
patent: 3566107 (1971-02-01), Taylor et al.
patent: 4804486 (1989-02-01), Hall
patent: 4873862 (1989-10-01), Scott et al.
patent: 4975648 (1990-12-01), Lawson et al.
patent: 5739699 (1998-04-01), Abdel-Rahman
patent: 5847494 (1998-12-01), Bayliss et al.

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