Measuring and testing – Liquid analysis or analysis of the suspension of solids in a... – Viscosity
Reexamination Certificate
2003-05-12
2004-11-23
Williams, Hezron (Department: 2856)
Measuring and testing
Liquid analysis or analysis of the suspension of solids in a...
Viscosity
C073S024060, C073S579000
Reexamination Certificate
active
06820469
ABSTRACT:
FIELD OF THE INVENTION
The present invention relates to flexural wave excitation and detection devices and, more particularly, to a microfabricated teeter-totter resonator.
BACKGROUND OF THE INVENTION
Surface acoustic wave and resonating devices have a number of applications, including frequency filtering, oscillator control, signal processing, and mass and load sensors. For example, microresonating devices can be used as filters to pass selective frequencies and provide frequency analysis of audible or ultrasonic signals. Acoustic devices can be used as a fluid monitor. Acoustic devices can also be used as gas and vapor chemical sensors.
Chemical sensors combine a chemically sensitive interface, which sorbs chemical species (i.e., analytes) from the environment, with a physical transducer that provides an electrical output proportional to the amount of sorbed species. Two commonly used acoustic devices for chemical sensing include surface acoustic wave (SAW) and resonant microsensors, such as the flexural plate wave (FPW) resonator. See S. J. Martin et al., “Gas Sensing with Acoustic Devices,”
Proc. IEEE Ultrasonics Symposium
, 423 (1996), which is incorporated herein by reference.
SAW sensors rely on the electrical excitation of a surface acoustic wave in a piezoelectric substrate. Typically, a wave is established on a quartz surface and the collection of analyte mass on the surface is reflected in the propagation of the surface wave. The high quality factor, Q, and low insertion loss of SAW chemical sensors makes them extremely stable in an oscillator circuit, resulting in low detection limits. SAW sensors can detect sub nanogram-levels of chemical analytes. However, SAW sensors typically operate at hundreds of megahertz frequencies, complicating the design and integration of oscillator circuitry.
A resonator comprises a vibrating element of a certain shape. Depending on the shape, the resonator can support several types of vibrations, e.g., longitudinal, transverse, torsional, and lateral, that can have a number of vibrational modes or resonances. The stress, mass, or shape of the resonator is typically designed such that one of these modes dominates and the resonant frequency of the dominant mode is matched to a driving excitation signal. When used as a chemical sensor, the collection of analyte mass on the surface of the resonator is reflected as a change in the resonant frequency or the amplitude of the vibration. The resonance change due to mass loading can also be used to detect changes in gas density and flows.
Resonators that operate on magnetic actuation principles are particularly attractive for many applications, due to their large dynamic range and high sensitivity. Electromagnetic sensors rely on a Lorentz force, generated by an alternating electrical current flowing in the resonator interacting with an external magnetic field, to excite a mechanical vibration in the structure.
A magnetically excited FPW (mag-FPW) resonator is described in S. J. Martin et al., “Flexural plate wave resonator excited with Lorentz forces,”
J. Appl. Phys
. 83(9), 4589 (1998) and U.S. Pat. No. 5,836,203, which are incorporated herein by reference. The mag-FPW resonator comprises current lines patterned on a silicon nitride membrane that is suspended on a silicon frame. A Lorentz force is created by the interaction of an alternating surface current flowing in the current lines and an in-plane static magnetic field perpendicular to the current flow direction. Preferential coupling to a particular membrane mode is achieved by positioning the current lines along antinodes of the longitudinal mode. When the alternating current has the natural frequency of the mag-FPW resonator, a large amplitude standing wave is set up in the membrane wave plate. The motion of the current conductor lines in the magnetic field in turn induces a back electromotive force (back-emf) opposing the motion. This back-emf can be detected as an increase in impedance of the current lines.
Because the confinement of kinetic energy is in a thin, low-mass membrane, the FPW sensor can have a very high mass sensitivity. Also, because the wave velocity in the FPW membrane is much less than in a solid substrate, the operating frequency of a FPW device is much lower than in a SAW device, resulting in simpler oscillator electronics. In addition, FPW resonators can be made with micromachining processes in a silicon wafer and can be integrated with microelectronic circuits. However, the temperature-dependent tension variation in the membrane, due to the differential thermal expansion of the silicon nitride membrane relative to the silicon frame, make the FPW operation very sensitive to temperature drift.
Therefore, a need remains for a microfabricated electromagnetic resonator having a high Q-factor, low operating frequency, high mass sensitivity, and low temperature drift. The microfabricated teeter-totter resonator of the present invention provides a Q-factor, operating frequency, and mass sensitivity comparable to the FPW resonators, but with much better temperature stability. In particular, the teeter-totter resonator is about three orders of magnitude less sensitive to temperature drift than the FPW resonator.
SUMMARY OF THE INVENTION
The present invention is directed to a microfabricated teeter-totter resonator, comprising a frame; a paddle having a first end and a second end and wherein the paddle is pivotably anchored to the frame by pivot arms at each end of the paddle, the pivot arms thereby defining an axis of rotation of the paddle; a current conductor line on a surface of the paddle that is displaced from the axis of rotation of the paddle; means for applying a static magnetic field aligned substantially in-plane with the paddle and substantially perpendicular to the current conductor line and the axis of rotation; and means for energizing the current conductor line with an alternating electrical current to excite an oscillatory motion of the paddle about the axis of rotation. The resonator can further comprise a means for detecting the oscillatory motion of the paddle. The resonator can further comprise a second current conductor line on a surface of the paddle for separate excitation and detection of the oscillatory motion of the paddle in a two-port device. For chemical sensing, the resonator can further comprise a chemically sensitive coating disposed on at least one surface of the paddle to sorb chemical analytes. Twin teeter-totters can be fabricated on the same frame to provide improved detection sensitivity and linearity when configured in a bridge circuit. The teeter-totter resonator can be fabricated with micromachining techniques with materials used in the integrated circuits manufacturing industry.
REFERENCES:
patent: 4248092 (1981-02-01), Vasile et al.
patent: 4567451 (1986-01-01), Greenwood
patent: 5836203 (1998-11-01), Martin et al.
patent: 6272907 (2001-08-01), Neukermans et al.
patent: 6387329 (2002-05-01), Lewis et al.
patent: 6397661 (2002-06-01), Grimes et al.
Grate, J.W., “Acoustic Wave Microsensor Arrays for Vapor Sensing,”Chem. Rev. 2000, 100, 2627-2648.
Martin, et al., “Gas Sensing with Acoustic Devices,”Proc. IEEE Ultrasonics Symposium, 423 (1996).
Martin et al., “Flexural plate wave resonator-excited with Lorentz forces,”J. Appl. Phys. 83(9), 4589 (1998).
Givens et al.., “A high Sensitivity, wide dynamic range magnetometer designed on a xylophone resonator,”Appl. Phys. Lett 69(18), 2755 (1996).
Adkins Douglas Ray
Heller Edwin J.
Shul Randy J.
Bieg Kevin W.
Saint-Surin Jacques M.
Sandia Corporation
Williams Hezron
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