Microencapsulated polymorphic agriculturally active material

Chemistry: fertilizers – Processes and products – Forms or conditioning

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71100, 71103, 71108, 71DIG1, A01N 3306, A01N 3720, A01N 3734, A01N 4106

Patent

active

051605309

ABSTRACT:
Agriculturally active materials, such as pesticides, herbicides and the like and a process for microencapsulating said materials. The present invention includes trifluralin having a polymorphic form characterized by a yellow color and a melting point of approximately 41.degree.-43.degree. C. The present invention also includes a method of using the yellow polymorphic form of trifluralin as a herbicide. In addition, the present invention includes a method of microencapsulating low-melting agriculturally active materials, such as trifluralin. The microencapsulation process comprises the steps of heating a low-melting, water-immiscible, agriculturally active material to a molten state. The molten active material is then combined with an aqueous soluion of a water-soluble, film-forming polymer at a temperature sufficient to maintain the active material in its molten state. The active material is then dispersed or emulsified in the aqueous solution so that the active material has a primary particle size of between approximately 0.1 and 10 microns. The resulting dispersion or emulsion is then spray dried at a temperature between approximately 50.degree. and 220.degree. C., so as to microencapsulate the active material in the polymer. Compounds for promoting the rapid solidification of the active material are also disclosed.

REFERENCES:
patent: 2800463 (1957-07-01), Morrison
patent: 3016308 (1962-01-01), Macaulay
patent: 3043782 (1962-07-01), Jensen
patent: 3112233 (1963-11-01), Friedman et al.
patent: 3159585 (1964-12-01), Evans et al.
patent: 3210208 (1965-10-01), Grass et al.
patent: 3293132 (1966-12-01), Stoyle et al.
patent: 3323922 (1967-06-01), Durst
patent: 3399069 (1968-08-01), Bridgeford
patent: 3429827 (1969-02-01), Ruus
patent: 3455838 (1969-07-01), Marotta et al.
patent: 3499962 (1970-03-01), Wurzburg et al.
patent: 3501419 (1970-03-01), Bridgeford
patent: 3501423 (1970-03-01), Tate et al.
patent: 3535423 (1970-10-01), Ordas
patent: 3556765 (1971-01-01), Houston
patent: 3574133 (1971-04-01), Bayless et al.
patent: 3577515 (1971-05-01), Vandegaer
patent: 3582495 (1971-06-01), Emrick
patent: 3584113 (1971-06-01), Takebe et al.
patent: 3627693 (1971-12-01), Scarpelli
patent: 3629140 (1971-12-01), Bayless et al.
patent: 3664963 (1972-05-01), Pasin
patent: 3778383 (1973-12-01), Schibler et al.
patent: 3780195 (1973-12-01), Balassa
patent: 3804775 (1974-04-01), Shiozaki et al.
patent: 3877928 (1975-04-01), Houston et al.
patent: 3883489 (1975-05-01), Matschke et al.
patent: 3927196 (1975-12-01), Hersh
patent: 3959464 (1976-05-01), DeSavigny
patent: 3971852 (1976-07-01), Brenner et al.
patent: 4011661 (1977-03-01), Sezaki et al.
patent: 4016254 (1977-04-01), Seager
patent: 4082537 (1978-04-01), Dudkowski
patent: 4144050 (1979-03-01), Frensch et al.
patent: 4150969 (1979-04-01), Dudkowski
patent: 4174960 (1979-11-01), Hendriksen
patent: 4244836 (1981-01-01), Frensch et al.
patent: 4280833 (1981-07-01), Beestman et al.
patent: 4286020 (1981-08-01), Himel et al.
patent: 4335260 (1982-06-01), Bornengo et al.
patent: 4353962 (1982-10-01), Himel et al.
patent: 4360376 (1982-11-01), Koestler
patent: 4415355 (1983-11-01), Cassell et al.
patent: 4417916 (1983-11-01), Beestman et al.
patent: 4439488 (1984-03-01), Trimnell et al.
patent: 4440746 (1984-04-01), Maglio
patent: 4440962 (1984-04-01), Pallucca
patent: 4501608 (1985-02-01), Cannon
patent: 4511395 (1985-04-01), Misselbrook
patent: 4537992 (1985-08-01), Pikarski et al.
patent: 4541860 (1985-09-01), Civilla et al.
patent: 4563212 (1986-01-01), Becher et al.
patent: 4622315 (1986-11-01), Dureja et al.
patent: 4640709 (1987-02-01), Beestman
patent: 4657582 (1987-04-01), Huber
patent: 4690786 (1987-09-01), Ninomiya et al.
patent: 4874425 (1989-10-01), Kimpara et al.
CA 106:183056x, Dumas, J. P., et al., "Phase Transformations in Emulsions. Part II. Polymorphism . . . ", J. Dispersion Sci. Technol., 1987, 8(1), 29-54.
Kondo, A., Microcapsule Processing and Technology, Chapters 1, 3, 4, 15, 1979.
"Applications of Spray Drying in Industry", pp. 528-531, 582-583, 611, 661-668, Attachment A, 1975.
Microencapsulation/Spray Drying, Abstracts, 1988.
Microencapsulation/PVA, Abstracts, 1988.
Encyclopedia of Polymer Science and Technology, vol. 14, 1972.
Goldschmiedt, Ph.D., "Microencapsulation", Soap/Cosmetics/Chemical Specialties for Sep. 1973, pp. 46-48.
Bakan, J. A. and Anderson, J. L., "Part III. Microencapsulation", The Theory and Practice of Industrial Pharmacy, 420, (2nd Ed. 1976), pp. 420-438.
Luzzi, L. A., "Microencapsulation", Journal of Pharmaceutical Sciences, vol. 59, No. 10, Oct. 1970.
Tsunemitsu, K. and Shohata, H., "Useful Properties and Industrial Uses of Polyvinyl Alcohol as a Water-Soluble Polymer", S.C.I. Monograph No. 30, pp. 104-129, no date.
Hackel, E., "Industrial Methods for the Preparation of Polyvinyl Alcohol", S.C.I. Monograph No. 30, pp. 1-15, 1965.
"Microencapsulation by Spray-Drying Process", (Attachment B), Chapter 15, pp. 154-165, 1979.
63-Pharmaceuticals, vol. 84, 79741h (1976).
37 Plastic Fab., Uses, vol. 83, col. 148614n (1975).
83 Chemical Abstracts, p. 276, col. 168481v (1975).
80 Chemical Abstracts, p. 42, col. 84172v (1974).
78 Chemical Abstracts, p. 262, col. 33916s (1973).
48 Unit Operations, Processes, vol. 77, p. 113, col. 128592b (1972).
37 Plastics Fabr., Uses, vol. 76, p. 41, col. 26106h (1972).
68 Chemical Abstracts, p. 2216, col. 22766k (1968).
36 Plastics Manufacture and Processing, vol. 66, p. 2849, col. 29562h (1967).
43 Organic Coatings and Inks, vol. 57, col. 8693a (1962).
43 Organic Coatings and Inks, vol. 56, col. 8878a (1962).
55 Chemical Abstracts, vol. 55, col. 26551b (1961).
37 Chemical Abstracts, vol. 37, col. 4536.sup.1 (1943).
63 Pharmaceutical, vol. 91, col. 162997m (1979).
109 Chemical Abstracts, p. 701, col. 83549(d) (1988).
37 Plastics Fabr., Uses 83 (148615p) (1975).
World Patent Search.

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