Methods of preparing polymer-organoclay composites and...

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – At least one aryl ring which is part of a fused or bridged...

Reexamination Certificate

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C524S442000, C524S492000

Reexamination Certificate

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07928154

ABSTRACT:
A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.

REFERENCES:
patent: 3383092 (1968-05-01), Cazier
patent: 3671487 (1972-06-01), Abolins
patent: 3723373 (1973-03-01), Lucas
patent: 3803085 (1974-04-01), Takehoshi et al.
patent: 3847867 (1974-11-01), Heath et al.
patent: 3850885 (1974-11-01), Takekoshi et al.
patent: 3852242 (1974-12-01), White
patent: 3855178 (1974-12-01), White et al.
patent: 3905942 (1975-09-01), Takekoshi et al.
patent: 3972902 (1976-08-01), Heath et al.
patent: 3983093 (1976-09-01), Williams, III et al.
patent: 4115341 (1978-09-01), Boldebuck et al.
patent: 4157996 (1979-06-01), Boldebuck et al.
patent: 4307226 (1981-12-01), Bolon et al.
patent: 4360633 (1982-11-01), Bolon et al.
patent: 4374972 (1983-02-01), Bolon et al.
patent: 4443591 (1984-04-01), Schmidt et al.
patent: 4455410 (1984-06-01), Giles, Jr.
patent: 4870194 (1989-09-01), Molinaro et al.
patent: 4957801 (1990-09-01), Maranci et al.
patent: 5021168 (1991-06-01), Molinaro et al.
patent: 5164460 (1992-11-01), Yano et al.
patent: 5229482 (1993-07-01), Brunelle
patent: 5260407 (1993-11-01), Saruwatari et al.
patent: 5460890 (1995-10-01), Okahashi et al.
patent: 5478915 (1995-12-01), Amone et al.
patent: 5707439 (1998-01-01), Takekoshi et al.
patent: 5807629 (1998-09-01), Elspass et al.
patent: 6028203 (2000-02-01), Brunelle et al.
patent: 6057035 (2000-05-01), Singh et al.
patent: 6117932 (2000-09-01), Hasegawa et al.
patent: 6232388 (2001-05-01), Lan et al.
patent: 6384121 (2002-05-01), Barbee et al.
patent: 6387996 (2002-05-01), Lan et al.
patent: 6410142 (2002-06-01), Chen et al.
patent: 6579927 (2003-06-01), Fischer
patent: 6653388 (2003-11-01), Barbee et al.
patent: 6906127 (2005-06-01), Liang et al.
patent: 2004/0127627 (2004-07-01), Gilmer et al.
patent: 2005/0234219 (2005-10-01), Silvi et al.
patent: 2005/0272847 (2005-12-01), Wang et al.
patent: 2007/0123682 (2007-05-01), Raj et al.
patent: 2007/0299186 (2007-12-01), Chan et al.
patent: 2007/0299187 (2007-12-01), Chan et al.
patent: 2007/0299188 (2007-12-01), Chan et al.
patent: 2007/0299189 (2007-12-01), Cao et al.
patent: 2008/0015330 (2008-01-01), Chan et al.
patent: 2008/0021175 (2008-01-01), Chan et al.
patent: 2008/0044639 (2008-02-01), Chan et al.
patent: 2008/0044682 (2008-02-01), Chan et al.
patent: 2008/0044683 (2008-02-01), Chan et al.
patent: 2008/0044684 (2008-02-01), Chan et al.
patent: 2009/0043024 (2009-02-01), Brunelle et al.
patent: 0178079 (1986-04-01), None
patent: 0459472 (1991-12-01), None
patent: 1350815 (2003-10-01), None
patent: 1473328 (2004-11-01), None
patent: 0078540 (2000-12-01), None
patent: WO 0078540 (2000-12-01), None
patent: WO 2005028363 (2005-03-01), None
Moy, et al., “Synthesis of Hydroxyl-Containing Polyimides Derived from 4,6-Diamino-Resorchinol Dihydrochloide and Aromatic Tetracarboxylic Dianhydrides,” Journal of Polymer Science: Part A: Polymer Chemistry, vol. 32, pp. 1903-1908 (Jul. 1994).
European Patent Office, PCT International Search Report, International Application No. PCT/US2007/071205, Date of Mailing: Oct. 21, 2008.
European Patent Office, PCT Written Opinion, International Application No. PCT/US2007/071205, Date of Mailing: Oct. 21, 2008.
Park, Cheol et al., “Polyimide/silica Hybrid-Clay Nanocomposites” Polymer vol. 46, No. 23 (Nov. 14, 2005) pp. 9694-9701, Elsevier Science Publishers, B.V.
International Search Report for PCT/US2007/072019 International Filing Date Jun. 25, 2007, Maling Date Jan. 8, 2008 (6 pages).
Written Opinion of the International Searching Authority for PCT/US2007/072019 International Filing Date Jun. 25, 2007, Mailing Date Jan. 8, 2008 (9 pages).
Lertwimolnun, W. et al. Polymer, 46, 3462, (2005).
Zhu, L. et al. J. of Applied Polymer Science, 93, 1891, (2004).
Lee, E. C. et al. Polymer Engineering and Science, 44, 1773, (2004).
Ton-That, M. -T. et al. Polymer Engineering and Science, 44, 1212, (2004).
Lam, C. et al. Materials Letters, 59, 1369, (2005).
Wang, J. et al. Ultrasonics Sonochemistry, 12, 165, (2005).
Yu, Z. et al. Journal of Polymer Science: Part B: Polymer Physics, 43, 1100, (2005).
Hasegawa, N. et al. Polymer, 44, 2933, (2003).
Dasari, A. et al. Composites Science and Technology, 65, 2314, (2005).
Kato, M. et al. Polymer Engineering and Science, 44, 1205, (2004).
Wang, K. et al. Langmuir, 21, 3613, (2005).
Chen, B. et al. Chemistry of Materials, 16, 4864, (2004).
Zhong, Y. et al. Polymer, 46, 3006, (2005).
Morgan, A. B. et al. Macromolecules, 34, 2735, (2001).
Park, J.H. et al. Macromolecules, 36, 2758, (2003).
Park, J.H. et al. Polymer, 45, 7673, (2004).
Paul, M.-A. et al. Macromolecular Chemistry and Physics, 206, 484, (2005).
Morgan, A.B. et al. Polymer, 45, 8695, (2004).
Chang, J. -H. et al. Polymer Engineering and Science, 41, 1514, (2001).
Ma, J. et al. Polymer, 44, 4619, (2003).
Jeon, H.S. et al. Polymer, 44, 5749, (2003).
Burgentzle, D. et al. J. of Colloid and Interface Science, 278, 26, (2004).
Perez-Maqueda, L.A. et al. Journal of the European Ceramic Society, 24, 2793, (2004).
JP2005298751, Polyester Resin Composition and Polyester Film, Publication Date: Oct. 27, 2005, Abstract, 1 page.
Panek, G. et al, “Heterogeneity of the Surfactant Layer in Organically Modified Silicates and Polymer-Layered Silicate Composites”, MACROMOLECULES, Feb. 28, 2006, p. 2191-2200, vol. 39, No. 6, American Chemical Society.
Sun, Xuehui et al, “Synthesis and Properties of Ionic, Rigid-Rod, and Thermally Stable Polymides Containing Bipyridinium Triflates”, MACROMOLECULES, 1998, p. 4291-4296, vol. 31, No. 13. American Chemical Society.
Burgentzle et al.; “Solvent-Based Nanocomposite Coatings I. Dispersion of Organophilic Montmorillonite in Organic Solvents”; Journal of Colloid and Interface Science; vol. 278 (2004); pp. 26-39.
Chang et al.; “Preparation and Characterization of Polyimide Nanocomposites with Different Organo-Montmorillonites”; Polymer Engineering and Science; vol. 41, No. 9 (Sep. 2001); pp. 1514-1520.
Chen et al.; “Synthesis of Disordered and Highly Exfoliated Epoxy/Clay Nanocomposites Using Organoclay with Catalytic Function via Acetone—Clay Slurry Method”; Chem. Matter; vol. 16 (2004); pp. 4864-4866.
Dasart et al.; “Clay Exfoliation and Organic Modification on Wear of Nylon 6 Nanocomposites Processed by Different Routes”; Composites Science and Technology; vol. 65 (2005); pp. 2314-2328.
Hasegawa et al.; “Nylon 6/Na-montmorillonite Nanocomposites Prepared by Compounding Nylon 6 with Na-montmorillonite Slurry”; Polymer; vol. 44 (2003); pp. 2933-2937.
Jeon et al.; “Characterization of Polyisoprene-Clay Nanocomposites Prepared by Solution Blending”; Polymer; vol. 44 (2003); pp. 5749-5758.
Kato et al.; “Development of New Production Method for a Polypropylene-Clay Nanocomposite”; Polymer Engineering and Science; vol. 44, No. 7 (Jul. 2004); pp. 1205-1211.
Lam et al.; “Effect of Ultrasound Sonication in Nanoclay Clusters of Nanoclay/Epoxy Composites”; Materials Letters; vol. 59 (2005); pp. 1369-1372.
Lee et al.; “Exfoliation and Dispersion Enhancement in Polypropylene Nanocomposites by In-Situ Melt Phase Ultrasonication&

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