Chemistry of inorganic compounds – Nitrogen or compound thereof – Binary compound
Patent
1987-09-11
1989-09-26
Doll, John
Chemistry of inorganic compounds
Nitrogen or compound thereof
Binary compound
C01B 2106
Patent
active
048698920
ABSTRACT:
A method of making fine particulate aluminum nitride, including the steps of reacting gaseous aluminum trichloride with aluminum-containing metallic material at elevated temperature to convert some of the trichloride to monochloride gas; introducing a gaseous nitrogen source to the monochloride-containing gas for reacting nitrogen with the monochloride to form fine particulate aluminum nitride; conducting a flow of gas comprising aluminum trichloride having the particulate nitride entrained therein to a cooling locality; there condensing the trichoride and accumulating the condensed trichloride and particulate nitride; and periodically reevaporating and removing the trichloride from the cooling locality for separating out and recovering the accumulated nitride.
REFERENCES:
patent: 3216820 (1965-11-01), Phillips et al.
patent: 3352637 (1967-11-01), Heymer et al.
patent: 3477812 (1969-11-01), Huml et al.
patent: 3607014 (1971-09-01), Huml et al.
patent: 3979500 (1976-09-01), Sheppard et al.
Chemical Abstracts, vol. 105, No. 26 (Dec. 1986), Abstract No. 229306p.
Raghavan Narasimha S.
Sood Raman R.
Southam Frederick W.
Alcan International Limited
Doll John
Lange Wayne A.
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