Methods for use of a sensitive layer for hydrogen sulphide...

Coating processes – Electrical product produced – Piezoelectric properties

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C422S083000

Reexamination Certificate

active

07867552

ABSTRACT:
Methods can be adapted for design of a sensitive monolayer for detection of hydrogen sulphide at room temperature with SAW/BAW devices. The sensitive monolayer can be synthesized based on chemical compounds, which belongs to a class of thiacalix[n]arenas, mercapto halides, mercapto alcohols and chloromethylated thiacalix[n]arenas. The sensitive monolayer can be directly immobilized or anchored at the surface of a piezoelectric quartz substrate in a covalently bonded manner by means of direct printing process. The piezoelectric quartz substrate can be activated in basic medium or in acid medium before the immobilization of the sensitive monolayer in order to increase the population of OH groups. Thus, the synthesized sensitive monolayer exhibits a high site density, fast response and long-term stability for H2S sensing.

REFERENCES:
patent: 6951690 (2005-10-01), Katz et al.
patent: 2008/0229831 (2008-09-01), Serban et al.
Sensing CO2 in a Chemically Modified Porous Silicon Film; M. Rocchia, E. Garrone, F. Geobaldo, L. Boarino, M.J. Sailor; Phys. Stat. Sol. (2) 197, No. 2, 365-369 (2003)/DOI 10, 1002/pssa.200306526.
Covalently Anchored Supramolecular Monolayers on Quartz Surfaces for Use in SAW Sensors; P. A. Lieberzeit, W. Greibl, H. Stathopulos, F.L. Dickert, G. Fisherauer, W. Bulst; Elsevier Science, Sensors and Actuators B 113 (2006) 677-683.
The First Single-Step Immobilization of a Calix-[4]-arene onto the Surface of Silica; A. Katz, P. D. Costa, A.C.P. Lam, J. M. Notestein; American Chemical Society, Chem. Mater. 2002, 14, 3364-3368.
Surface Acoustic Wave Microsensors Based on Cyclodextrin Coatings; D. Li, M. Ma; Elsevier Science, Sensors and Actuators B 69 (2000) 75-84.
Recent Advances in the Functionalizations of The Upper Rims of Thiacalix[4]Arenes. A Review.; S. Parola, C. Desroches; Collect. Czech. Chem. Commun. (vol. 69 (2004).
Upper Rim Substituted Thiacalix[4]Arenes; O. Kasyan, D. Swierczynski, A. Drapailo, K. Suwinska, J. Lipkowski, V. Kalchenko; Science Direct, Tetrahedron Letters 44 (2003) 7167-7170.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Methods for use of a sensitive layer for hydrogen sulphide... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Methods for use of a sensitive layer for hydrogen sulphide..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Methods for use of a sensitive layer for hydrogen sulphide... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-2713931

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.