Methods for selectively recovering vanadium from phosphoric acid

Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Group vb metal

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423 67, 423321R, C01G 3102

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active

049785117

ABSTRACT:
Vanadium is selectively recovered from vanadium-containing phosphoric acid solutions also containing metals other than vanadium by selectively converting the dissolved vanadium to a vanadate compound insoluble in the phosphoric acid solution and separating the resulting insoluble vanadate compound, free of other metal compounds, from the phosphoric acid solution. The dissolved vanadium can be converted to an insoluble vanadate by reaction with oxidants and/or cations which form phosphoric acid-insoluble vanadates. These methods can be employed to selectively recover vanadium from phosphoric acid solutions containing other metals. They also can be employed to recover vanadium compounds from ores, scrap metal, and other vanadium sources by dissolving the vanadium from the vanadium source in phosphoric acid and recovering the vanadium as an insoluble compound from the phosphoric acid as described. Alternatively, the vanadium can be dissolved in a strong acid other than phosphoric acid, and sufficient phosphoric acid can be added to the resulting solution to ensure selective precipitation of impurity-free vanadates by the procedure described above.

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