Methods for producing N-(8-[2-hydroxybenzoyl]-amino)...

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

Reexamination Certificate

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C560S039000, C564S134000

Reexamination Certificate

active

07544833

ABSTRACT:
Disclosed are improved methods for the synthesis of N-(8-[2-hydroxybenzoyl]-amino)caprylic acid. Certain compounds have been found useful for preventing the formation of a colored impurity when included in an ester hydrolysis reaction. Conducting ester hydrolysis in anaerobic conditions has also been found to minimize the formation of the color impurity. Also disclosed are improved methods for synthesizing the sodium salt of N-(8-[2-hydroxybenzoyl]-amino)caprylic acid.

REFERENCES:
patent: 3840570 (1974-10-01), Julian
patent: 4927814 (1990-05-01), Gall et al.
patent: 5650386 (1997-07-01), Leone-Bay et al.
patent: WO 00/46182 (2000-08-01), None
patent: WO 00/59863 (2000-10-01), None
patent: WO 01/70219 (2001-09-01), None

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