Methods for preparing 7alpha-hydroxy-dehydroepiandrosterone

Organic compounds -- part of the class 532-570 series – Organic compounds – Cyclopentanohydrophenanthrene ring system containing

Reexamination Certificate

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Reexamination Certificate

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06930192

ABSTRACT:
The invention relates to new processes for preparing 7alpha-hydroxy-dehydroepiandrosterone of formula (1):

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P. Marwah et al.: “Steroidal allylic fluorination using diethylaminosulfur trifluoride: A convenient method for the synthesis of 3beta-acetoxy-7alpha- and 7beta-fluoroandrost-5-en-17-one” Steroids: Structure, Function, and Regulation, vol. 61, No. 8, pp. 453-460, Aug. 1, 1996.
Jar Salvador et al.: “Copper catalysed allylic oxidation of DELTA-steroids by t-butyl hydroperoxide” Tetrahedron Letters, vol. 38, No. 1, pp. 119-122 Jan. 6, 1997.
V. Pouzar et al.: “Synthesis of (19E)-3beta, 7alpha-dihydroxy-17oxoandrost-5-en-19-al 19-(0-carboxymethyl)oxime, a new hapten for 7alpha-hydroxydehydroepiandrosterone(3beta,7alpha-dihydroxyandrost-5-en-17-one)—7alpha-hydroxylation of dehydroepiandrosterone and pregnenolone by rat brain microsomes” Steroids: Structure, Function, and Regulation, vol. 63, No. 9, pp. 454-458, Sep. 1, 1998.

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