Methods for evaluating and manufacturing rubber and method...

Chemistry: analytical and immunological testing – Synthetic or natural resin

Reexamination Certificate

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C264S040100, C264S236000, C264S328200

Reexamination Certificate

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08076146

ABSTRACT:
A method for evaluating rubber is provided which can evaluate the degree of crosslinking of a crosslinked rubber product within a short period of time without performing any specific treatment. In the above method, the amount of energy shift of the peak (such as the peak of C12p3/2 of chlorinated butyl rubber) of a constituent element of the rubber is measured by photoelectron spectroscopy, and the degree of crosslinking of the rubber is evaluated from the amount of energy shift. In addition, a method for manufacturing a rubber product is also provided which includes the steps of measuring the amount of energy shift of the peak of a constituent element of the rubber product by a photoelectron spectrometer which is installed in a manufacturing line and then feeding back measurement result to adjust heat molding conditions so as to obtain a desired degree of crosslinking.

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Hitsuda et al. Kinetics of the reactions of CI(2P1/2) and C1(2P3/2) atoms with C2H6, C2D6, CHF3, C2H5F, and CH3CF3 at 298 K. The Journal of Physical Chemistry A. vol. 105. pp. 5131-5136. (May 4, 2001).

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