Methods and compositions relating to the reduction of...

Earth boring – well treating – and oil field chemistry – Preventing contaminant deposits in petroleum oil conduits

Reexamination Certificate

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Details

C507S128000, C507S269000, C507S271000, C507S274000, C507S276000

Reexamination Certificate

active

07989397

ABSTRACT:
This invention relates to methods and compositions useful in treating crude sources, and more specifically, to methods and compositions useful in reducing the concentration of phosphorus in crude streams and hydrocarbon flowback fluids. In some embodiments, the present invention provides methods that include a method comprising: providing a crude stream or a hydrocarbon flowback fluid; optionally testing the crude stream or the hydrocarbon flowback fluid for total phosphorus content; optionally testing the crude stream or hydrocarbon flowback fluid for volatile phosphorus content; adding a solution comprising a trivalent metal ion to the crude stream or the hydrocarbon flowback fluid; adding a sufficient amount of a caustic solution to the crude stream or the hydrocarbon flowback fluid to raise the pH of the stream or the fluid to about 8 or more; allowing at least a plurality of precipitates to form; removing at least one precipitate; and forming a clean crude stream or a clean hydrocarbon flowback fluid.

REFERENCES:
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patent: 3865922 (1975-02-01), Boontje
patent: 4080311 (1978-03-01), Kehl
patent: 4927614 (1990-05-01), Langer
patent: 6133205 (2000-10-01), Jones
patent: 6511944 (2003-01-01), Taylor et al.
patent: 7314850 (2008-01-01), Taylor et al.
patent: 2004/0214728 (2004-10-01), Taylor et al.
patent: 2007/0173413 (2007-07-01), Lukocs et al.

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