Methods and apparatus for analysis of complex mixtures

Measuring and testing – Sampler – sample handling – etc. – With heating or cooling

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

73 2341, 7386484, G01N 3054

Patent

active

059708042

ABSTRACT:
This invention provides methods and apparatus for determining the presence or absence of a specific constituent in a mixture. A thermal desorption unit includes a body providing a desorption chamber, a removable end cap for closing the chamber, a desorber heating system arranged to heat the desorption chamber, a gas inlet to the desorption chamber, and a gas outlet from the desorption chamber. A valve assembly can operate in a run mode to direct a carrier gas to the thermal desorption unit gas inlet, and couple the thermal desorption unit gas outlet to an inlet of a sample analysis instrument. The valve assembly also can operate in a flush mode to direct the carrier gas to the inlet of the gas analysis instrument, direct a flushing gas to the thermal desorption unit gas inlet, and couple the thermal desorption unit gas outlet to an exhaust.

REFERENCES:
patent: 2826180 (1958-03-01), Lupfer et al.
patent: 3733908 (1973-05-01), Linenberg
patent: 4128008 (1978-12-01), Linenberg
patent: 4344917 (1982-08-01), Schorno
patent: 4376391 (1983-03-01), Brunnee
patent: 4707603 (1987-11-01), Miemela et al.
patent: 4980131 (1990-12-01), Meuzelaar et al.
patent: 4982097 (1991-01-01), Slivon et al.
patent: 5072115 (1991-12-01), Zhou
patent: 5175430 (1992-12-01), Enke et al.
patent: 5247175 (1993-09-01), Schoen et al.
patent: 5285064 (1994-02-01), Willoughby
patent: 5400665 (1995-03-01), Zhu et al.
patent: 5440119 (1995-08-01), Labowsky
patent: 5453613 (1995-09-01), Gray et al.
patent: 5475612 (1995-12-01), Espinosa et al.
patent: 5481476 (1996-01-01), Windig
patent: 5588988 (1996-12-01), Gerstel et al.
Abraham et al., "Data Comparison Study Between Field and Laboratory Detection of Polychlorinated Biphenyls and Polycyclic Aromatic Hydrocarbons at Superfund Sites," Haz. Waste & Haz. Mat., 461-473 (1993) vol. 10, No. 4 month not given.
Bendl et al., "MS-UTIL: a program for interpretation and manipulation of mass spectra and chemical structures," Comput. Methods Programs Biomed. 46:23-28 (1995) month not given.
Lareau et al., "Peak Identification for Mass Spectroscopy," Surface and Interface Analysis, 17:38-42 (1991) month not given.
Robbat et al., "Evaluation of a Thermal Desorption Gas Chromatograph/Mass Spectrometer: On-Site Detection of Polychlorinated Biphenyls at a Hazardous Waste Site," Analytical Chemistry 358-364 vol. 64, No. 4 Feb. 15, 1992.
Robbat et al., "On-Site Detection of Polycyclic Aromatic Hydrocarbons in Contaminated Soils by Thermal Desorption Gas Chromatography/Mass Spectrometry," Analytical Chemistry 1477-1483 vol. 64, No. 13 Jul. 1, 1992.
Stauffer et al., "Probability-Based-Matching Algorithm with Forward Searching Capabilities for Matching Unknown Mass Spectra of Mixtures," Anal. Chem. 1056-1060 vol. 57, No. 6, May 1985.
Steiger et al., Automated peak interpretation in low-resolution SIMS spectra; a comparison of two algorithms, Vacuum 321-327 (1983) vol. 33, No. 6, month not given.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Methods and apparatus for analysis of complex mixtures does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Methods and apparatus for analysis of complex mixtures, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Methods and apparatus for analysis of complex mixtures will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-751507

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.