Method to reveal microstructures in single phase alloys

Chemistry: analytical and immunological testing – Process or composition for determination of physical state... – Surface area – porosity – imperfection – or alteration

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73104, 75 05R, 156664, 356 36, 436 73, 436164, G01N 2188, G01N 3320

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045489033

ABSTRACT:
A method for revealing the microstructure of metal alloys which comprises the steps of polishing the sample, chemically etching the polished metal surface, thermally etching the chemically etched surface and quenching the thermally etched sample. This method allows observation of deformed and recrystallized grains on the same polished surface and provides the opportunity to correlate recrystallized grains to their nucleation sites.

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Eylon, "The Microscope", vol. 23, 3rd Quarter, 1975, pp. 133-137.
Voort, "Metallography Principles & Practice", 1984, McGraw Hill Book Co., N.Y., pp. 185-186.
F. H. Froes, J. M. Capenos and C. F. Yoltan, "Decoration of Plastically Strained Regions in Metallic Systems", Metallography, 9, 1976, pp. 535-537.
E. D. Hondros and A. J. W. Moore, "Thermal Etching of Silver Surfaces Parallel to [110] Planes", Acta. Met., 7, 1959, pp. 521-523.
W. B. Morrison, "Recrystallization of a Low-Carbon Steel in the Austenite Range", Draft of Paper Intended for Publication in JISI, Aug. 1971.

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