Method of varying the temperature of a tube bundle reactor

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including heat exchanger for reaction chamber or reactants...

Reexamination Certificate

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C422S198000, C422S198000, C422S186220, C422S198000, C165S061000, C165S104320

Reexamination Certificate

active

07988927

ABSTRACT:
A method of varying the temperature of a tube bundle reactor for catalytic gas phase reactions upon start-up and shut-down, the tube bundle reactor comprising a major reactor portion which includes a bundle of vertically disposed reactor tubes, upper and lower tubesheets tightly connected to the upper and lower ends, respectively, of the reactor tubes, and a reactor shell enclosing the tube bundle, a heat transfer medium having a melting temperature in the range of from 100° C. to 450° C. flowing around the outer surfaces of the reactor tubes during normal operation and being circulated in at least one circuit through the major reactor portion, comprising the steps: (a) varying the heat transfer medium temperature during circulation of the heat transfer medium; and (b) passing a temperature gas through the reactor tubes at least when the heat transfer medium is not yet or no longer circulated.

REFERENCES:
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patent: 2004007064 (2004-01-01), None
Stankiewicz, Chem.Eng.Technol. 1989, 12, pp. 113-130.
European Search Report; Application No. EP07014486; dated Jan. 21, 2010; 4 pages.

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