Method of synthesizing Mo.sub.3 S.sub.x containing compounds

Solid anti-friction devices – materials therefor – lubricant or se – Lubricants or separants for moving solid surfaces and... – Nitrogen and heavy metal – or nitrogen and aluminum – in the...

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556 38, 556 57, C10M13900, C07F 1100

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active

059069686

ABSTRACT:
A method of making an oil-soluble or oil-dispersible trinuclear molybdenum-sulfur compound, comprising: reacting two to less than three equivalents of a tetrahydrocarbyl thiuram disulfide and one equivalent of trinuclear molybdenum compound of the formula Mo.sub.3 S.sub.x (L).sub.4 wherein x is from 4 to 10 and L is dihydrocarbyl-dithiocarbamate.

REFERENCES:
patent: 5631213 (1997-05-01), Tanaka et al.
patent: 5688748 (1997-11-01), Tomizawa
Shibahara, "Synthesis of Sulphur-Bridged Molybdenum and Tungsten Coordination Compounds," Coordination Chemistry Reviews, 123 (1993), 73-147.

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