Method of stabilizing chelated polyvalent metal solutions

Chemistry of inorganic compounds – Sulfur or compound thereof – Elemental sulfur

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423224, 423226, 423573G, 423578R, 210764, 422 28, 422 35, 422 36, 422 37, C01B 1704, B01D 5334

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active

044552874

ABSTRACT:
An aqueous oxidation-reduction composition and method for removing hydrogen sulfide gas from a fluid stream by liquid phase oxidation of the hydrogen sulfide to elemental sulfur with a chelated polyvalent metal catalyst, such as iron, wherein the composition is stabilized against rapid loss of chelated polyvalent catalyst caused by contamination of the aqueous composition with micro-organisms, such as bacteria. The aqueous composition is stabilized by incorporating in the aqueous composition and adding throughout the normal usage thereof a broad spectrum biocide in an amount which acts as a bacteriostat to prevent rapid growth of bacteria in the aqueous composition and when the bacteria concentration rises above about 1.times.10.sup.6 colonies per ml. slug-feeding in a kill concentration into the aqueous composition while the chelated polyvalent metal catalyst is being contacted with oxygen a fast acting broad spectrum biocide, such as 2,2-dibromo-2-cyanoacetamide or glutaraldehyde, and thereafter resuming addition of the first mentioned biocide.

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