Method of stabilized operation of acid digestion kettle of tanta

Chemical apparatus and process disinfecting – deodorizing – preser – Process disinfecting – preserving – deodorizing – or sterilizing – Maintaining environment nondestructive to metal

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241DIG38, 252626, 422 3, 422 9, 422 12, C23F 1104, C23F 1118

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045870985

ABSTRACT:
A method of minimizing corrosion deterioration and hydrogen absorption embrittlement of tantalum encountered in performing acid digestion of organic waste matter put in an acid digestion kettle of tantalum containing high temperature high concentration sulfuric acid includes the addition of nitric acid, nitrous acid, nitrates, nitrites and/or nitrogen oxides to the sulfuric acid bath.

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Stern, M. and C. Bishop, 1963, "Corrosion and Electrochemical Behavior", In: Sisco and Epremian, Columbium and Tantalum, John Wiley and Sons, New York, pp. 304-312, 579-596.
Tantulum: Acid-Proof Process Equipment, Dec. 1937, Fansteel Metallurgical Corporation, Chicago, Illinois, 33 pages.

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