Mineral oils: processes and products – Fractionation – Liquid extraction with solvents
Patent
1991-09-26
1993-10-12
Morris, Theodore
Mineral oils: processes and products
Fractionation
Liquid extraction with solvents
208322, 208326, C10G 2120, C10G 2112
Patent
active
052522008
ABSTRACT:
The process for separating an aromatic from an entry hydrocarbon mixture also containing nonaromatics, by an extractive distillation method using an extractive distillation column with a selective solvent consisting essentially of an N-substituted Morpholine having substituents each of which contain no more than seven carbon atoms, includes distilling off the nonaromatics from the top of the extractive distillation column as a top product, drawing the aromatic and selective solvent from the extractive distillation column and subsequently separating the selective solvent from the aromatic in a separator column. The extractive distillation column is provided with an additional column portion for separation of a selective solvent residue from the separated nonaromatics without a separate top product distillation column. The hydrocarbon entry mixture is heated prior to admission to the extractive distillation column by an indirect heat exchange with selective solvent drawn from the separator column and heated to a temperature of from 130.degree. to 150.degree. C. to form a heated entry hydrocarbon mixture.
REFERENCES:
patent: 2455803 (1948-12-01), Pierotti
patent: 3591490 (1971-07-01), Muller et al.
patent: 4519901 (1985-05-01), Fiocco
patent: 4595491 (1986-06-01), Berns
patent: 4664783 (1987-05-01), Preusser et al.
Schneider Hans-Christoph
Skatulla Luzian
Vollmer Hans-Jurgen
Griffin Walter D.
Krupp Koppers GmbH
Morris Theodore
Striker Michael J.
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