Method of removing oxygen from a controlled atmosphere

Chemistry of inorganic compounds – Modifying or removing component of normally gaseous mixture – Molecular oxygen or ozone component

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423579, 4235801, 502 3, 502407, 2521815, 252194, 2521816, C01B 1300

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active

053405536

ABSTRACT:
A method is provided for removing residual amounts of oxygen and water vapor from the controlled atmosphere of an enclosed chamber. A small volume of high-purity silicon is heated in a crucible placed inside the chamber. The silicon is typically heated with a power source separate from that used for heating the chamber and its primary contents. The heated silicon functions as an effective oxygen getter for removing residual oxygen and water vapor from the controlled atmosphere before and/or during a process conducted in the chamber. Heating the silicon to a molten state can induce beneficial convective stirring that keeps the silicon surface fresh for effective, efficient, and continuous capturing of oxygen.

REFERENCES:
patent: 2469435 (1949-05-01), Hirsch
patent: 3241217 (1966-03-01), Nunn
patent: 3704806 (1972-12-01), Plachenov et al.
patent: 4081397 (1978-03-01), Booe
patent: 4516984 (1985-05-01), Warner et al.
patent: 4563368 (1986-01-01), Tihanyi et al.
patent: 4906595 (1990-03-01), van der Plas et al.
patent: 5135548 (1992-08-01), Golden et al.
"Vapor Deposition of Silicon Dioxide" by D K Seto et al; IBM Technical Disclosure Bulletin vol. 9 No. 7 Dec. 1966.

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