Method of removing oligomers from olefin monomer vapor in the po

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Removing and recycling removed material from an ongoing...

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526 77, C08F 600, C08F 1000

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active

040680606

ABSTRACT:
Removing oligomers (short chain polymers of from two to seven atoms in the chain) from olefin monomer vapor recovered for recycle from the reaction mass resulting from the catalytic polymerization of liquid olefinic monomers by flowing such recovered vapor through a mass transfer plate tower upwardly through openings in the plates of said tower and in the form of bubbles through layers of liquid oligomer reflux maintained on said plates by weirs and downcomers by means of which said reflux is flowed from each plate downwardly to the plate below it and, as a layer, along the top of the plate and thence downwardly to the next lower plate, condensing in a reflux condenser the vapor from the top of said tower, removing olefin monomer from said condenser as a vapor and refluxing condensed liquid oligomers back to the top of said tower. Preferably the tower is a valve tray tower and the plates are valve trays.

REFERENCES:
patent: 3255171 (1966-06-01), Eilbracht et al.
patent: 3403080 (1968-09-01), Clay
patent: 3523929 (1970-08-01), Paige et al.
patent: 3634300 (1972-01-01), Fischer et al.
patent: 3770709 (1973-11-01), Tegge et al.
patent: 3953301 (1976-04-01), Mendez et al.

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