Method of recovering and purifying diphenylcarbonate from phenol

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbonate esters

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558270, C07C 6996

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active

052391060

ABSTRACT:
Phenolic solutions of 20%-70% by weight of diphenylcarbonate have been found to form a crystalline 1:1 molar adduct of diphenylcarbonate and phenol when allowed to cool to a temperature between about 50.degree. C. and 25.degree. C. Recovery of the crystalline 1:1 molar adduct followed by distillation of phenol therefrom has been found to provide substantially pure diphenylcarbonate.

REFERENCES:
patent: 3251873 (1966-05-01), Kurkjy et al.
patent: 4013702 (1977-03-01), Cartier et al.

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