Method of purifying lithium hexafluorophosphate

Details Method of purifying lithium hexafluorophosphate Method of purifying lithium hexafluorophosphate

2005-04-26

2005-04-26

Langel, Wayne A. (Department: 1754)

Chemistry of inorganic compounds

Phosphorus or compound thereof

Halogen containing

Reexamination Certificate

active

06884403

ABSTRACT:
A method of purifying lithium hexafluorophosphate that allows to purify lithium hexafluorophosphate, useful as lithium secondary cell electrolyte, organic synthesis medium or the like, to an extremely high purity is provided. Lithium hexafluorophosphate containing harmful impurities such as oxyfluoride, lithium fluoride is purified by adding phosphoric chloride. The purification is performed in the presence of phosphoric chloride and hydrogen fluoride of the quantity equal or superior to the equivalent amount for reacting them, and then by converting lithium fluoride lithium hexafluorophosphate with generated phosphor pentafluoride.

REFERENCES:
patent: 5866093 (1999-02-01), Belt et al.
patent: 6514474 (2003-02-01), Kikuyama et al.
patent: 298507 (1994-10-01), None

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