Method of purifying crude 2,6-naphthalenedicarboxylic acid dimet

Distillation: processes – separatory – Vaporization zone under positive pressure or vacuum

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203 7, 560 80, 560 78, B01D 310

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active

040480216

ABSTRACT:
In a method of obtaining purified 2,6-naphthalenedicarboxylic acid dimethyl ester by vacuum distilling crude 2,6-naphthalenedicarboxylic acid dimethyl ester under conditions of application of heat, the improvement which comprises vacuum distilling a crude 2,6-naphthalenedicarboxylic acid dimethyl ester having an acid value (A.sub.f), as expressed in milligrams of KOH required for neutralizing the carboxyl groups contained in one gram of said crude 2,6-naphthalenedicarboxylic acid dimethyl ester, of from 1.0 to 50.

REFERENCES:
patent: 2938837 (1960-05-01), Meyer et al.
patent: 3382271 (1968-05-01), McNerney
patent: 3517053 (1970-06-01), Antonsen
patent: 3639451 (1972-02-01), Ebert
patent: 3818071 (1974-06-01), Chilton
Perry's Chemical Engineer's Handbook; McGraw-Hill; 4th Edition; pp. 2-87 to 2-90.

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