Method of purification of the oxalic acid diamide

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564125, C07B 6300, C07C10314

Patent

active

050684299

ABSTRACT:
A method of removing copper from oxamide obtained through a process which involves the use of copper catalysts, by contacting it with an aqueous solution of a suitable complexing agent, which is capable of forming copper-containing water-soluble complexes and imparts to the aqueous solution a pH comprised between 2 and 8, optionally repeating the contacting step and, finally, recovering the purified oxamide by solid-liquid separation techniques.
The claimed process affords oxamide containing less than 25 ppm of copper.

REFERENCES:
patent: 3776957 (1973-12-01), Newkirk
patent: 3989753 (1976-11-01), Riemenschneider et al.

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