Method of producing reinforced aqueous emulsion of polydiorganos

Details Method of producing reinforced aqueous emulsion of polydiorganos Method of producing reinforced aqueous emulsion of polydiorganos

1985-05-24

1987-04-28

Ivy, C. Warren

Synthetic resins or natural rubbers -- part of the class 520 ser

Synthetic resins

At least one aryl ring which is part of a fused or bridged...

524837, C08L 8306

Patent

active

046615563

ABSTRACT:
This invention is a method of producing a colloidal silica reinforced polydiorganosiloxane fluid in aqueous emulsion. The method combines an acidic aqueous colloidal silica sol and low molecular weight hydroxyl endblocked polydiorganosiloxane with anionic emulsifying agent, then homogenizes the mixture to form an emulsion. Because the water in the colloidal silica sol is used to supply water for the emulsion, it is possible to produce emulsions with solid content as high as 80 percent by weight. The emulsion is then mixed with surface active anionic catalyst and aged at room temperature to allow the polydiorganosiloxane to polymerize. Polymerization is halted by adding base to bring the pH to greater than 7. The reinforced polydiorganosiloxane emulsion can be further mixed with diorganotindicarboxylate and aged to give a curable emulsion which yields an elastomer upon removal of the water. A curable emulsion can also be produced by mixing the reinforced polydiorganosiloxane emulsion with diorganotindicarboxylate and alkylorthosilicate.

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