Method of producing nitrile compounds

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitriles

Reexamination Certificate

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C558S438000, C558S439000

Reexamination Certificate

active

08039660

ABSTRACT:
The present invention relates to the manufacture of nitrile compounds from unsaturated organic compounds by reaction with hydrogen cyanide. It relates more particularly to the manufacture of nitrile compounds of use in the synthesis of adiponitrile, an important chemical intermediate in the manufacture of major chemical compounds, such as hexamethylenediamine and ε-caprolactam. The invention provides a process for the manufacture of organic compounds comprising at least one nitrile functional group by carrying out a hydrocyanation reaction between hydrogen cyanide and an organic compound comprising at least one ethylenic unsaturation. This reaction is carried out in the presence of a catalytic system comprising a metal element chosen from the group consisting of nickel, platinum and palladium and an organophosphorus ligand, the reaction medium additionally comprising an ionic liquid in the liquid state at least at the temperature at which the hydrocyanation reaction is carried out.

REFERENCES:
patent: 4087452 (1978-05-01), Kuntz
patent: 6197992 (2001-03-01), Fischer et al.
patent: 6469194 (2002-10-01), Burattin et al.
patent: 6559344 (2003-05-01), Mackewitz
patent: 2004/0260112 (2004-12-01), Basset et al.
patent: 2 338 253 (1977-08-01), None
patent: 2 739 378 (1997-04-01), None
patent: 2 787 446 (2000-06-01), None
patent: 2 829 763 (2001-09-01), None
patent: WO 00 32572 (2000-06-01), None
International Search Report for PCT/FR02/03166 dated Nov. 28, 2002.

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