Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material
Patent
1983-05-12
1984-05-15
Bascomb, Jr., Wilbur L.
Distillation: processes, separatory
With chemical reaction
Including step of adding catalyst or reacting material
203 75, 203 76, 203 77, 203DIG13, 203DIG19, 568921, B01D 340, C07C 2988
Patent
active
044486448
ABSTRACT:
This invention relates to a process for purifying crude ethanol, whether produced by fermentation or by the synthetic route, to produce a pure ethanol-water azeotrope. The process uses only two distillation columns for fermentation ethanol or synthetic ethanol eventhough the latter has diethyl ether as impurity. The inventive concept lies in the design and specification of the columns and the specific high pressure and low reflux ratio distillation conditions which enable each of the impurities in ethanol to be reduced below ppm. Ethanol of such purity is most desirable when used for potable or pharmaceutical purposes.
REFERENCES:
patent: 2801209 (1957-07-01), Muller et al.
patent: 3265594 (1966-08-01), DeJean et al.
patent: 3406100 (1968-10-01), Karafian
patent: 3445345 (1969-05-01), Katzen et al.
patent: 4308109 (1981-12-01), Griffiths et al.
Foster Brian R.
Woodfin William T.
Bascomb, Jr. Wilbur L.
BP Chemicals Limited
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