Method of producing aqueous latex of crosslinked polydiorganosil

Details Method of producing aqueous latex of crosslinked polydiorganosil Method of producing aqueous latex of crosslinked polydiorganosil

1985-05-24

1986-10-21

Ivy, C. Warren

Synthetic resins or natural rubbers -- part of the class 520 ser

Synthetic resins

At least one aryl ring which is part of a fused or bridged...

524837, 521154, C08K 541, C08K 542, C08L 8314

Patent

active

046186450

ABSTRACT:
A method of producing an emulsion of crosslinked polydiorganosiloxane admixes hydroxyl endblocked polydiorganosiloxane, alkoxy silicone compound, anionic emulsifying agent, and water. The mixture is homogenized, then the emulsion is admixed with surface active anionic catalyst. Maintaining the catalyzed emulsion, having a pH of less than 5, at room temperature allows the ingredients to react to raise the molecular weight of the polydiorganosiloxane and to crosslink the polymer. The reaction is halted by adding sufficient base to raise the pH to greater than 7. The resultant latex yields an elastomer upon removal of the water. When colloidal silica is also added to the mixture before homogenization, the final latex yields a reinforced elastomer upon removal of the water.

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