Method of producing a silver halide photographic emulsion, appar

Radiation imagery chemistry: process – composition – or product th – Including control feature responsive to a test or measurement

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430569, G03K 1015

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active

057028516

ABSTRACT:
A method of producing a silver halide photographic emulsion in which a silver ion concentration in precipitation of a silver halide emulsion in a precipitation bath is controlled, wherein a precipitation bath in which stirring is conducted rapidly and uniformly, and crystal formation and crystal growth are uniformly performed is used, the method comprises the steps of: in a start period of precipitation, quantitavely adding a silver nitrate solution and a halogen salt solution at a constant ratio flow rate; when an E.sub.Ag value reaches a designated E.sub.Ag value region in the vicinity of a preset target E.sub.Ag value, starting a control of an adding rate of the halogen salt solution by using a controller which has an operation period equal to or shorter than 1 sec.; and after holding a tuning parameter of a proportional, integral and differential (PID) action controller to a minimum response level, conducting a control in which the tuning parameter is switched to an optimum control tuning parameter which corresponds to the preset target value and a solute rate of silver/halogen ions to be added.

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Quantitative Kinetic Study of Crystal Growth, I. Effect of Dilution on Crystal Growth durig the Precipitation of Silver Bromide in Gelatin, Claes et al., Photographische Korrespondenz, Nr. 1208 der ganzen Folge, Nr. Mar. 1965, pp.37-42.
Photographic Emulsion Chemistry, G.F. Duffin, The Focal Press, London & New York, pp. 12-15.

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