Method of producing 1,1,1,3,3-pentafluoropropane, a method of pr

Organic compounds -- part of the class 532-570 series – Organic compounds – Halogen containing

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570228, C07C 1708

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057637059

ABSTRACT:
There are provided production methods of 1,1,1,3,3-pentafluoropropane characterized in that 1,1,1,3,3-pentafluoro-2,3-dichloropropane is reacted with hydrogen fluoride in the presence of a noble metal catalyst; of 1,1,1,3,3-pentafluoro-2-halogeno-3-chloropropane characterized in that the halogenated propene indicated as general formula I is fluorinated in the presence of antimony trihalogenide and/or antimony pentahalogenide by hydrogen fluoride of mole ratio of or over five times the said antimony halogenide in a liquid phase; and of 1,1,1,2,3,3-hexachloropropene characterized in that 1,1,1,2,2,3,3-heptachloropropane is reacted with an aqueous solution of alkali metal hydroxide in the presence of a phase transfer catalyst. Therefore, an industrial manufacturing method which is possible to obtain the objective product easily at low cost and high yield can be provided.

REFERENCES:
patent: 2637747 (1953-05-01), McBee
patent: 2724004 (1955-11-01), Frederick
patent: 2942036 (1960-06-01), Smith et al.
patent: 3639493 (1972-02-01), Campbell
patent: 4980324 (1990-12-01), Kellner et al.
patent: 5447896 (1995-09-01), Rao

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