Method of preparing purified alkanesulfonic acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfonic acids or salts thereof

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562118, 562119, 562115, C07C 6100

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active

055832539

ABSTRACT:
A process of preparing purified alkanesulfonic acid from crude aqueous alkanesulfonic acid containing oxidizable impurities wherein the crude material is treated with a sufficient amount of chlorine to convert the oxidizable impurities to alkanesulfonyl chloride and then hydrolyzing said alkanesulfonyl chloride to alkanesulfonic acid by heating.

REFERENCES:
patent: 3626004 (1971-12-01), Guertin
patent: 4450047 (1984-05-01), Malzahn
patent: 4699736 (1987-10-01), Gongora et al.
patent: 4859373 (1989-08-01), Olliver et al.
patent: 4895977 (1990-01-01), Nosowitz
patent: 4938846 (1990-07-01), Comstock et al.
Chemical Abstracts, vol. 79, No. 3, 23 Jul. 1973, Columbus, Ohio, U.S.A., Abstract No. 18083 v, p. 402 1990 R. Oda et al. "Methanesulfonic Acid".
Chemical Abstracts, vol. 79, p. 402--item 18083v., Jul. 1973 (Abstract of Japan Kokai 73 22423).

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