Method of preparing pressureless sintered, highly dense...

Plastic and nonmetallic article shaping or treating: processes – Outside of mold sintering or vitrifying of shaped inorganic... – Utilizing binder to add green strength to preform

Reexamination Certificate

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Reexamination Certificate

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07919040

ABSTRACT:
In a method of preparing a boron carbide material, boron carbide powder is washed with essentially pure water at an elevated temperature to generate washed boron carbide powder. The washed boron carbide powder is combined with a sintering aid. The mixture of the boron carbide powder and the sintering aid is pressed to form a shaped material, and the shaped material is sintered. A sintered boron carbide material comprises a boron carbide component that includes boron carbide, elemental carbon, and not more than about 0.6 wt % of oxygen on the basis of the total weight of the boron carbide component. The sintered boron carbide material has a density of at least about 99% of the theoretical density. Another sintered boron carbide material comprises a boron carbide component that includes boron carbide, silicon carbide, elemental carbon, and not more than about 0.3 wt % oxygen on the basis of the total weight of the boron carbide component, and has a density of at least about 97% of the theoretical density.

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Lee, H. and Speyer, R.F., “Hardness and Fracture Toughness of Pressureless-Sintered Boron Carbide (B4C),”J. Am. Ceram. Soc., 85(5): 1291-1293 (May 2002).
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Notification Concerning Transmittal of International Preliminary Report on Patentability (Chapter 1 of the Patent Cooperation Treaty) for Int'l Application No. PCT/US2008/009484; Date Mailed: Feb. 18, 2010.

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