Method of preparing hydrophobic precipitated silica

Coating processes – Particles – flakes – or granules coated or encapsulated – Inorganic base

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427221, 4274432, 106490, B05D 310

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active

059086602

ABSTRACT:
A method for the preparation of hydrophobic precipitated silicas which are useful, for example, as reinforcing fillers in rubber compositions. The method comprises two steps, where in the first step an aqueous suspension of precipitated silica is contacted with an organosilicon compound in the presence of a catalytic amount of an acid to effect hydrophobing of the precipitated silica. In the second step the aqueous suspension of the hydrophobic precipitated silica is contacted with a water-immiscible organic solvent at a solvent to silica weight ratio greater than 5:1 to effect separation of the hydrophobic precipitated silica from the aqueous phase.

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Zumbrum, Acid/base properties of fumed silica fillers used in silicone elastomers; Adhes. Soc., Proc. Sixteenth Annu. Meet. Int. Symp. Interphase (1993), pp. 140-142.

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