Method of preparing dimethylamine-borane

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564 8, C07F 502

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055656153

ABSTRACT:
In the preparation of dimethylamine-borane by reacting an alkali metal or alkaline earth metal borohydride with a dimethylammonium salt, the improvement which comprises effecting the reaction in a liquid mixture comprising dimethylamine as a solvent and an additional organic solvent.

REFERENCES:
patent: 4709083 (1987-11-01), Spielvogel
Y. Kikugona, Chem. Pharm Bull. vol. 35, pp. 4988-4989 (1987).
North et al. Chemische Berichte, vol. 3, pp. 928-938 (1960).
Derwent Abstract of JP 60-149,593 (Jan. 12, 1989).
Hawthorne, JACS, 2671-2673, 1961.

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